tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate
CAS No.:1228827-92-6
Molecular Formula:C₃₂H₃₇IN₂O₅
Molecular Weight:656.561
Hs Code.:

Synonyms:tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

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Chemical Property of tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

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Technology Process of tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

There total 1 articles about tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1228827-54-0
tert-butyl 2-{5-[2-(4-(methoxymethoxy)phenyl)ethoxy]-1H-indole-3-yl}ethylcarbamate

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 1228827-92-6
tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

Guidance literature:: tert-butyl 2-{5-[2-(4-(methoxymethoxy)phenyl)ethoxy]-1H-indole-3-yl}ethylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h; Inert atmosphere;

1-bromomethyl-4-iodobenzene; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.04.001

Reference yield:

: 1228827-92-6
tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

: 5720-07-0
4-methoxyphenylboronic acid

: C₃₉H₄₄N₂O₆

Guidance literature:: With palladium diacetate; caesium carbonate; In 1,4-dioxane; water; for 4h; Reflux;
DOI:10.1016/j.bmc.2010.04.001

Reference yield:

: 1228827-92-6
tert-butyl 2-{5-[4-(methoxymethoxy)phenethyloxy]-1-(4-iodo-benzyl)-1H-indole-3-yl}ethylcarbamate

: 1423-26-3
(meta-(trifluoromethyl)phenyl)boronic acid

: C₃₉H₄₁F₃N₂O₅

Guidance literature:: With palladium diacetate; caesium carbonate; triphenylphosphine; In 1,4-dioxane; water; for 4h; Reflux;
DOI:10.1016/j.bmc.2010.04.001