2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

Base Information

Chemical Name:2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine
CAS No.:126797-57-7
Molecular Formula:C₁₇H₁₆N₂OS
Molecular Weight:296.393
Hs Code.:

Synonyms:2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

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Chemical Property of 2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

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Technology Process of 2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

There total 2 articles about 2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 103-72-0
phenyl isothiocyanate

: 126797-54-4
N-(trimethylsilyl)-2-(1-oxabut-3-enyl)benzylideneamine

: 126797-57-7
2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

Guidance literature:: With water; In toluene; at 90 ℃; for 10h;
DOI:10.1039/c39890001487

Reference yield:

: 28752-82-1
2-(allyloxy)benzaldehyde

: 126797-57-7
2-(phenylimino)-1,2,3,4,4a,10b-hexahydro-5H-<1>benzopyrano<4,3-d><1,3>thiazine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-BuLi, 1,1,1,3,3,3-hexamethyldisilazane / 1) hexane, THF, 30 min, 0 deg C, 2) 30 min

2: 2) water / 1) toluene, 10h, 90 deg C

With n-butyllithium; water; 1,1,1,3,3,3-hexamethyl-disilazane;
DOI:10.1021/jo00019a040