C₂₇H₂₉ClO₉

Base Information

• Chemical Name: C₂₇H₂₉ClO₉
• CAS No.: 1443342-36-6
• Molecular Formula: C₂₇H₂₉ClO₉
• Molecular Weight: 532.975
• Mol file: 1443342-36-6.mol

Synonyms:C₂₇H₂₉ClO₉

Chemical Property of C₂₇H₂₉ClO₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₇H₂₉ClO₉

There total 5 articles about C₂₇H₂₉ClO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H31ClO9 (1443341-94-3) → C27H29ClO9 (1443342-36-6)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

dapagliflozin (461432-26-8,1373321-04-0) → C27H29ClO9 (1443342-36-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap / pyridine / 20 °C / Cooling with ice

1.2: 3 h / 20 °C

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; boron trifluoride diethyl etherate; Dess-Martin periodane; In pyridine; dichloromethane;

Reference yield:

C33H45ClO8Si → C27H29ClO9 (1443342-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; Dess-Martin periodane; In dichloromethane;

upstream raw materials:

dapagliflozin

C₂₇H₃₁ClO₉