5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

Base Information

Chemical Name:5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide
CAS No.:820965-31-9
Molecular Formula:C₁₆H₂₁ClF₃N₃O₃
Molecular Weight:395.809
Hs Code.:

Synonyms:5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

There total 1 articles about 5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 364-62-5
metoclopramide

: 407-25-0
trifluoroacetic anhydride

: 820965-31-9
5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

Guidance literature:: With triethylamine; In chloroform;
DOI:10.1016/0223-5234(96)88294-8

Reference yield: 100.0%

: 820965-31-9
5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

: C₁₆H₂₁ClF₃N₃O₄

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; Ambient temperature;
DOI:10.1016/0223-5234(96)88294-8

Reference yield:

: 820965-31-9
5-Chloro-N-(2-diethylamino-ethyl)-2-methoxy-4-(2,2,2-trifluoro-acetylamino)-benzamide

: 171367-22-9
metoclopramide N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / m-chloroperbenzoic acid / CHCl₃ / Ambient temperature

2: 100 percent / aq. Na₂CO₃ / methanol / Ambient temperature

With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform;
DOI:10.1016/0223-5234(96)88294-8