Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester
• CAS No.: 204527-47-9
• Molecular Formula: C₂₀H₃₁I₂NO₆
• Molecular Weight: 635.278
• Mol file: 204527-47-9.mol

Synonyms:Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

Chemical Property of Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

There total 4 articles about Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C34H45NO12S2 (204527-46-8) → Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester (204527-47-9)

Guidance literature:

With sodium iodide; In acetone; for 12h; Heating;

DOI:10.3891/acta.chem.scand.52-0374

Reference yield:

3,6,12,15-tetraoxa-9-azaheptadecane-1,17-diol (25743-12-8) → Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester (204527-47-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / ethanol / 12 h / Ambient temperature

2: 80 percent / DMAP, pyridine / CH₂Cl₂ / 12 h / Ambient temperature

3: 98 percent / NaI / acetone / 12 h / Heating

With pyridine; dmap; potassium carbonate; sodium iodide; In ethanol; dichloromethane; acetone;

DOI:10.3891/acta.chem.scand.52-0374

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → Bis-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester (204527-47-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / ethanol / 12 h / Ambient temperature

2: 80 percent / DMAP, pyridine / CH₂Cl₂ / 12 h / Ambient temperature

3: 98 percent / NaI / acetone / 12 h / Heating

With pyridine; dmap; potassium carbonate; sodium iodide; In ethanol; dichloromethane; acetone;

DOI:10.3891/acta.chem.scand.52-0374

upstream raw materials:

C₃₄H₄₅NO₁₂S₂

3,6,12,15-tetraoxa-9-azaheptadecane-1,17-diol

benzyl chloroformate

Bis-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester