2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

Base Information

Chemical Name:2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester
CAS No.:908371-36-8
Molecular Formula:C₂₉H₂₂N₄O₃
Molecular Weight:474.519
Hs Code.:

2'-(2-benzyloxy-phenyl)-1<i>H</i>,1'<i>H</i>-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

Synonyms:2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

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Technology Process of 2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

There total 15 articles about 2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 908371-35-7
2-amino-3-{[2-(2-benzyloxy-phenyl)-1H-benzoimidazole-4-carbonyl]-amino}-benzoic acid methyl ester

: 908371-36-8
2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

Guidance literature:: With acetic acid; at 120 - 130 ℃; for 2h;
DOI:10.1016/j.bmc.2006.05.007

Reference yield:

: 95067-27-9
2-acetylamino-3-nitro-benzoic acid methyl ester

: 908371-36-8
2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methoxide / methanol / 20 °C

2: 96 percent / hydrogen / Pd/C / methanol / 3 h

3: 0.27 g / triethylamine / CH₂Cl₂ / 20 °C

4: 85 percent / acetic acid / 2 h / 120 - 130 °C

With hydrogen; sodium methylate; acetic acid; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2006.05.007

Reference yield:

: 2719-08-6
methyl 2-(acetylamino)benzoate

: 908371-36-8
2'-(2-benzyloxy-phenyl)-1H,1'H-[2,4']bibenzoimidazolyl-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acetic anhydride; acetic acid; nitric acid / 2.5 h / 5 - 15 °C

2: sodium methoxide / methanol / 20 °C

3: 96 percent / hydrogen / Pd/C / methanol / 3 h

4: 0.27 g / triethylamine / CH₂Cl₂ / 20 °C

5: 85 percent / acetic acid / 2 h / 120 - 130 °C

With hydrogen; nitric acid; sodium methylate; acetic anhydride; acetic acid; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2006.05.007