C₂₄H₃₀O₄

Base Information

Chemical Name:C₂₄H₃₀O₄
CAS No.:1232773-05-5
Molecular Formula:C₂₄H₃₀O₄
Molecular Weight:382.5
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:C₂₄H₃₀O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₀O₄

Chemical Property:

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Technology Process of C₂₄H₃₀O₄

There total 4 articles about C₂₄H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 140-10-3
(E)-3-phenylacrylic acid

: 1232773-08-8
C₁₅H₂₄O₃

: 1232773-05-5
C₂₄H₃₀O₄

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 23 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ja201921j

Reference yield:

: 1292771-15-3
C₈H₁₃ClO₂

: 1232773-05-5
C₂₄H₃₀O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 23 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: -78 - 23 °C / Inert atmosphere

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 3 h / 23 °C / Inert atmosphere

4.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 48 h / 23 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; samarium diiodide; 2,4,6-trichlorobenzoyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; diisopropylamine; In tetrahydrofuran; toluene; 2.1: Michael addition / 2.2: Michael addition;
DOI:10.1021/ja201921j

Reference yield:

: 25579-24-2
5-Isopropyl-2-methyl-furan-3-one

: 1232773-05-5
C₂₄H₃₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 23 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 3 h / 23 °C / Inert atmosphere

3.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 48 h / 23 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; samarium diiodide; 2,4,6-trichlorobenzoyl chloride; triethylamine; diisopropylamine; In tetrahydrofuran; toluene; 1.1: Michael addition / 1.2: Michael addition;
DOI:10.1021/ja201921j