C₂₂H₂₁ClN₂O₃S

Base Information

Chemical Name:C₂₂H₂₁ClN₂O₃S
CAS No.:1609070-60-1
Molecular Formula:C₂₂H₂₁ClN₂O₃S
Molecular Weight:428.939
Hs Code.:

C<sub>22</sub>H<sub>21</sub>ClN<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₂H₂₁ClN₂O₃S

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Chemical Property of C₂₂H₂₁ClN₂O₃S

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Technology Process of C₂₂H₂₁ClN₂O₃S

There total 4 articles about C₂₂H₂₁ClN₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609070-59-8
C₂₈H₂₅ClN₂O₄S₂

: 1609070-60-1
C₂₂H₂₁ClN₂O₃S

Guidance literature:: C₂₈H₂₅ClN₂O₄S₂; With pyridine; phosphorus pentachloride; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With methanol; In dichloromethane; at -40 - 0 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 80366-21-8
diphenylmethyl 7-(2-thienylacetamido)-2,3-dimethylenecepham-4-carboxylate

: 1609070-60-1
C₂₂H₂₁ClN₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -40 °C / Inert atmosphere

3.1: phosphorus trichloride / N,N-dimethyl-formamide / 0.5 h / -50 - -20 °C / Inert atmosphere

4.1: phosphorus pentachloride; pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.2: 0.5 h / -40 - 0 °C / Inert atmosphere

With pyridine; hydrogenchloride; phosphorus pentachloride; 3-chloro-benzenecarboperoxoic acid; phosphorus trichloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 87263-06-7
(6R,7R)-3-Chloromethyl-4-methyl-8-oxo-7-(2-thiophen-2-yl-acetylamino)-5-thia-1-aza-bicyclo[4.2.0]oct-3-ene-2-carboxylic acid benzhydryl ester

: 1609070-60-1
C₂₂H₂₁ClN₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -40 °C / Inert atmosphere

2.1: phosphorus trichloride / N,N-dimethyl-formamide / 0.5 h / -50 - -20 °C / Inert atmosphere

3.1: phosphorus pentachloride; pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.2: 0.5 h / -40 - 0 °C / Inert atmosphere

With pyridine; phosphorus pentachloride; 3-chloro-benzenecarboperoxoic acid; phosphorus trichloride; In dichloromethane; N,N-dimethyl-formamide;