5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

Base Information

• Chemical Name: 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide
• CAS No.: 583844-04-6
• Molecular Formula: C₃₀H₃₆N₂O₈
• Molecular Weight: 552.624

Synonyms:5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

Chemical Property of 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

Chemical Property:

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Technology Process of 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

There total 1 articles about 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-03-5) + benzyl bromide (100-39-0) → C30H36N2O8 + 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-04-6)

Guidance literature:

3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.25h;

benzyl bromide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 7h;

Reference yield: 12.0%

C30H36N2O8 + 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH2O-acetonide (583844-04-6) → 5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine (583844-05-7)

Guidance literature:

With methanol; at 20 ℃; for 8h; Heating / reflux;

upstream raw materials:

3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine 3'-O,3'-C-CH₂O-acetonide

benzyl bromide

Downstream raw materials:

5'-O-benzyl-3-N-benzyloxymethyl-3'-C,4'-C-bis(hydroxymethyl)thymidine

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