3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

Base Information

Chemical Name:3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide
CAS No.:947530-70-3
Molecular Formula:C₂₃H₂₆BrNO₄
Molecular Weight:460.368
Hs Code.:

Synonyms:3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

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Chemical Property of 3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

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Technology Process of 3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

There total 4 articles about 3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1033812-01-9
C₁₆H₁₅O₇N

: 947530-52-1
[2-(2-bromophenyl)ethyl]isopropylamine

: 947530-70-3
3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1021/ol071079g

Reference yield:

: 4698-21-9
3-(3,4,5-trimethoxyphenyl)propiolic acid

: 947530-70-3
3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / dioxane / 20 °C

2: 72 percent / dioxane / 20 °C

With dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ol071079g

Reference yield:

: 65185-58-2
2-(2-bromophenyl)ethanamine

: 947530-70-3
3-(3,4,5-trimethoxyphenyl)propynoic acid [2-(2-bromophenyl)ethyl]isopropylamide

Guidance literature:: Multi-step reaction with 3 steps

1: CD₂Cl₂ / 2 h / 20 °C

2: 847 mg / NaBH(OAc)3 / 1,2-dichloro-ethane

3: 72 percent / dioxane / 20 °C

With sodium tris(acetoxy)borohydride; In 1,4-dioxane; dichloromethane-d2; 1,2-dichloro-ethane;
DOI:10.1021/ol071079g