methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside
CAS No.:155480-22-1
Molecular Formula:C₃₁H₃₆O₅
Molecular Weight:488.624
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

There total 1 articles about methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2622-05-1
allylmagnesium bromide

: 73111-14-5
3,4,5-tris(benzyloxy)-2-(bromomethyl)-6-methoxytetrahydro-2H-pyran

: 155480-22-1
methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

Guidance literature:: In tetrahydrofuran; hexane; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo702663w

Reference yield: 72.0%

: 155480-22-1
methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

: 1021954-31-3
C₃₀H₃₄O₆

Guidance literature:: methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside; With ozone; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; at -78 - 20 ℃; for 4h; Further stages.;
DOI:10.1021/jo702663w

Reference yield:

: 155480-22-1
methyl 2,3,4-tri-O-benzyl-6,7,8,9-tetradeoxy-α-D-gluco-non-8-enopyranoside

: (2R,3S,4R)-2,3,4-Tris-benzyloxy-4-((2R,5S)-5-iodomethyl-tetrahydro-furan-2-yl)-butyraldehyde

: (2R,3S,4R)-2,3,4-Tris-benzyloxy-4-((2R,5R)-5-iodomethyl-tetrahydro-furan-2-yl)-butyraldehyde

Guidance literature:: With iodonium di(2,4,6-trimethylpyridine) perchlorate; water; In dichloromethane; Yield given. Yields of byproduct given. Title compound not separated from byproducts;