N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Base Information

Chemical Name:N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine
CAS No.:1453169-60-2
Molecular Formula:C₄₉H₆₉Cl₃N₂O₁₈Si
Molecular Weight:1108.53
Hs Code.:

N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Synonyms:N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

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Chemical Property of N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

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Technology Process of N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

There total 1 articles about N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1453169-59-9
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-3-O-(9-fluorenylmethoxycarbonyl)-6-O-tert-butyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)-amino-β-D-glucosamine

: 1453169-60-2
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.201300664

Reference yield:

: 1304695-84-8
C₁₉H₂₆O₆S

: 1453169-60-2
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

: N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-β-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

: 1453169-61-3
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 ℃; for 0.25h; Overall yield = 81%; Overall yield = 0.47 g; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201300664