N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Base Information

Chemical Name:N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine
CAS No.:1453169-61-3
Molecular Formula:C₆₆H₈₉Cl₃N₂O₂₄Si
Molecular Weight:1428.88
Hs Code.:

N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Synonyms:N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Suppliers and Price of N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

There total 1 articles about N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1304695-84-8
C₁₉H₂₆O₆S

: 1453169-60-2
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

: N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-β-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

: 1453169-61-3
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 ℃; for 0.25h; Overall yield = 81%; Overall yield = 0.47 g; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201300664

Reference yield: 87.0%

: 1453169-61-3
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-6-O-allyloxycarbonyl-β-D-galactopyranose-(1→4)-6-O-tertbutyldimethylsilyl-3-O-3,4-di-O-acetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)amino-β-D-glucosamine

: 1453169-62-4
N-benzyloxycarbonyl-5-aminopentyl 2,3-di-O-acetyl-4-O-benzyl-β-D-galactopyranose-(1→4)-6-O-tert-butyldimethylsilyl-3-O-3,4-di-Oacetyl-2-O-benzyl-α-L-fucose-(1→3)-2-deoxy-(2,2,2-trichloroethyloxycarbonyl)-amino-β-D-glucosamine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.201300664