2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine

Base Information

• Chemical Name: 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine
• CAS No.: 195191-36-7
• Molecular Formula: C₅₁H₇₈N₄O₃
• Molecular Weight: 795.205
• Mol file: 195191-36-7.mol

Synonyms:2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine

Chemical Property of 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine

There total 1 articles about 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-di-tert-butyl-2-hydroxybenzaldehyde (37942-07-7) + triethylentetramine (112-24-3) → 2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine (195191-36-7)

Guidance literature:

In methanol; for 2h;

DOI:10.1039/c3dt51095f

Reference yield: 65.0%

2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine (195191-36-7) + benzyl alcohol (100-51-6,185532-71-2) → [(2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine(3-))Mg2(benzyl alcohol(1-))]

Guidance literature:

2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine; With dibutylmagnesium; In hexane; toluene; at 0 ℃; for 3h; Inert atmosphere;

benzyl alcohol; In hexane; toluene; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c5dt01784j

Reference yield: 64.0%

2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine (195191-36-7) + diethylzinc (557-20-0) + benzyl alcohol (100-51-6,185532-71-2) → [(2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine(3-))Zn2(benzyl alcohol(1-))]

Guidance literature:

2-(3,5-di-tert-butyl-2-hydroxyphenyl)-1,3-bis[4-(3,5-di-tert-butyl-2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine; diethylzinc; In hexane; toluene; at 0 ℃; for 3h; Inert atmosphere;

benzyl alcohol; In hexane; toluene; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c5dt01784j

upstream raw materials:

3,5-di-tert-butyl-2-hydroxybenzaldehyde

triethylentetramine