trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

Base Information

Chemical Name:trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone
CAS No.:55311-78-9
Molecular Formula:C₂₁H₂₈O₈
Molecular Weight:408.449
Hs Code.:

Synonyms:trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

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Chemical Property of trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

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Technology Process of trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

There total 4 articles about trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3066-90-8
2,3-dimethoxy-5-methylbenzene-1,4-diol

: 66855-36-5
(E)-diethyl 2-(4-acetoxy-2-methylbut-2-en-1-yl)malonate

: 55311-78-9
trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane;
DOI:10.1248/cpb.26.774

Reference yield:

: 32659-14-6
4-bromo-3-methyl-2-buten-1-ol acetate

: 55311-78-9
trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Na, benzene, (ii) /BRN= 2237207/

2: BF₃-Et₂O / dioxane

With boron trifluoride diethyl etherate; In 1,4-dioxane;
DOI:10.1248/cpb.26.774

Reference yield:

: 105-53-3
diethyl malonate

: 55311-78-9
trans,cis-2,3-Dimethoxy-5-methyl-6-(5',5'-diethoxycarbonyl-3'-methyl-2'-pentenyl)-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Na, benzene, (ii) /BRN= 2237207/

2: BF₃-Et₂O / dioxane

With boron trifluoride diethyl etherate; In 1,4-dioxane;
DOI:10.1248/cpb.26.774