(2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

Base Information

Chemical Name:(2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester
CAS No.:872092-12-1
Molecular Formula:C₁₅H₂₅NO₄
Molecular Weight:283.368
Hs Code.:

Synonyms:(2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

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Chemical Property of (2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

There total 2 articles about (2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 68735-62-6
cyclohexen-1-en-3-yl diethyl phosphate

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 872092-12-1
(2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

Guidance literature:: N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester; With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

With lithium chloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

cyclohexen-1-en-3-yl diethyl phosphate; In N,N-dimethyl-formamide; at -30 - 20 ℃; for 16h;
DOI:10.1039/b512784j

Reference yield:

: 822-67-3
Cyclohex-2-enol

: 872092-12-1
(2S)-2-tert-butoxycarbonylamino-3-cyclohexen-2'-enyl-propanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 60 percent / pyridine / CH₂Cl₂ / 16 h / 0 - 20 °C

2.1: Zn; TMSCl / dimethylformamide / 0.33 h / 0 °C

2.2: CuCN; LiCl / dimethylformamide / 0.08 h / 0 °C

2.3: 40 percent / dimethylformamide / 16 h / -30 - 20 °C

With pyridine; chloro-trimethyl-silane; zinc; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b512784j