3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

Base Information

Chemical Name:3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine
CAS No.:77628-10-5
Molecular Formula:C₂₁H₂₄N₂O₃S
Molecular Weight:384.499
Hs Code.:

Synonyms:3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

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Chemical Property of 3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

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Technology Process of 3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

There total 1 articles about 3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 77628-11-6
6L-amino-3D-benzhydryloxycarbonyl-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine p-toluenesulfonic acid salt

: 77628-10-5
3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

Guidance literature:: With sodium hydrogencarbonate; In ethyl acetate;
DOI:10.1139/v81-062

Reference yield:

: 77628-10-5
3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

: 77628-17-2
(1R,3S,6R)-6-((S)-5-Benzhydryloxycarbonyl-5-tert-butoxycarbonylamino-pentanoylamino)-2,2-dimethyl-1,5-dioxo-1λ⁴-[1,4]thiazepane-3-carboxylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / 1.) ethyl acetate, 5 min; 2.) 72 h

2: 98 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.5 h / 0 °C

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1139/v81-062

Reference yield:

: 77628-10-5
3D-benzhydryloxycarbonyl-6L-amino-2,2-dimethyl-5-oxoperhydro-1,4-thiazepine

: 77628-18-3
(1R,3S,6R)-6-[(S)-5-Benzhydryloxycarbonyl-5-(2-tert-butoxycarbonylamino-acetylamino)-pentanoylamino]-2,2-dimethyl-1,5-dioxo-1λ⁴-[1,4]thiazepane-3-carboxylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / 1.) ethyl acetate, 5 min; 2.) 72 h

2: 1.) p-TsOH / 1.) methylene chloride, ether, reflux, 10 h; 2.) 20 h, r.t.

3: 91 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.33 h / 2 °C

With toluene-4-sulfonic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1139/v81-062