2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

Base Information

Chemical Name:2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper
CAS No.:1257343-10-4
Molecular Formula:C₄₉H₃₄CuN₄O₂
Molecular Weight:774.381
Hs Code.:

Synonyms:2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

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Chemical Property of 2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

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Technology Process of 2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

There total 1 articles about 2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1257343-59-1,158239-95-3,158342-00-8,940948-89-0
2-(2-formylvinyl)-5,10,15,20-tetraphenylporphyrinatocopper

: 107-21-1
ethylene glycol

: 1257343-10-4
2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

Guidance literature:: 2-(2-formylvinyl)-5,10,15,20-tetraphenylporphyrinatocopper; ethylene glycol; With toluene-4-sulfonic acid; In 1,4-dioxane; benzene; for 7h; Reflux;

With orthoformic acid triethyl ester; In 1,4-dioxane; benzene; for 2h; Reflux;
DOI:10.1134/S1070428010090241

Reference yield: 81.0%

: 1257343-10-4
2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper

: 1257343-13-7
2-[2-(1,3-dioxolan-2-yl)ethyl]-5,10,15,20-tetraphenylporphyrinatocopper

Guidance literature:: 2-[2-(1,3-dioxolan-2-yl)vinyl]-5,10,15,20-tetraphenylporphyrinatocopper; With oxygen; hydrazine; In pyridine; at 20 ℃; for 240h; Darkness;

With chloranil; In toluene; for 26h; Reflux;

With potassium hydroxide; In water; toluene; at 20 ℃; for 8h;
DOI:10.1134/S1070428010090241