C₄₅H₇₁NO₄

Base Information

• Chemical Name: C₄₅H₇₁NO₄
• CAS No.: 1459809-76-7
• Molecular Formula: C₄₅H₇₁NO₄
• Molecular Weight: 690.063
• Mol file: 1459809-76-7.mol

Synonyms:C₄₅H₇₁NO₄

Chemical Property of C₄₅H₇₁NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₇₁NO₄

There total 6 articles about C₄₅H₇₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-Ethynylaniline (14235-81-5) + 3,4,5-tris(((S)-3,7-dimethyloctyl)oxy)benzoic acid (798567-90-5) → C45H71NO4 (1459809-76-7)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1002/anie.201704294

Reference yield: 80.0%

4-Ethynylaniline (14235-81-5) + C39H70O5 → C45H71NO4 (1459809-76-7)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1039/c3cc44997a

Reference yield:

p-aminoiodobenzene (540-37-4) → C45H71NO4 (1459809-76-7)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 12 h / 40 °C / Inert atmosphere

2: potassium hydroxide / tetrahydrofuran; methanol / 12 h / 35 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 48 h / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1039/c3cc44997a

upstream raw materials:

4-Ethynylaniline

p-aminoiodobenzene

methyl 3,4,5-tris[(S)-3,7-dimethyloctyloxy]benzoate

3,4,5-tris(((S)-3,7-dimethyloctyl)oxy)benzoic acid