C₄₈H₆₁N₉O₁₂

Base Information

Chemical Name:C₄₈H₆₁N₉O₁₂
CAS No.:1632161-63-7
Molecular Formula:C₄₈H₆₁N₉O₁₂
Molecular Weight:956.065
Hs Code.:

C<sub>48</sub>H<sub>61</sub>N<sub>9</sub>O<sub>12</sub>

Synonyms:C₄₈H₆₁N₉O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₆₁N₉O₁₂

Chemical Property:

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Technology Process of C₄₈H₆₁N₉O₁₂

There total 5 articles about C₄₈H₆₁N₉O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 908341-15-1
N-[3-[[[(2S)-2-amino-3-methylbutanoyl]amino]carbamoyl]-4-methoxyphenyl]acetamide

: 1632161-96-6
4,4'-(3-aminonaphthalene-2,7-diyl)bis(oxy)dibutanoic acid

: 1632161-63-7
C₄₈H₆₁N₉O₁₂

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c4md00032c

Reference yield:

: 102653-36-1
3-bromonaphthalene-2,7-diol

: 1632161-63-7
C₄₈H₆₁N₉O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 50 °C

2: potassium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; Benzophenone imine / 1,4-dioxane / 15 h / 110 °C / Schlenk technique; Inert atmosphere

3: hydrogen; palladium on carbon / methanol; ethyl acetate / 24 h / 20 °C

4: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

With Benzophenone imine; palladium on carbon; hydrogen; palladium diacetate; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; ethyl acetate; N,N-dimethyl-formamide; 2: |Buchwald-Hartwig Coupling;
DOI:10.1039/c4md00032c

Reference yield:

: 1632161-74-0
benzyl 4-[[7-(4-benzyloxy-4-oxo-butoxy)-6-bromo-2-naphthyl]oxy]butanoate

: 1632161-63-7
C₄₈H₆₁N₉O₁₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; Benzophenone imine / 1,4-dioxane / 15 h / 110 °C / Schlenk technique; Inert atmosphere

2: hydrogen; palladium on carbon / methanol; ethyl acetate / 24 h / 20 °C

3: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

With Benzophenone imine; palladium on carbon; hydrogen; palladium diacetate; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; ethyl acetate; N,N-dimethyl-formamide; 1: |Buchwald-Hartwig Coupling;
DOI:10.1039/c4md00032c