C₃₀H₃₈N₆O₅

Base Information

Chemical Name:C₃₀H₃₈N₆O₅
CAS No.:1401533-33-2
Molecular Formula:C₃₀H₃₈N₆O₅
Molecular Weight:562.669
Hs Code.:

C<sub>30</sub>H<sub>38</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:C₃₀H₃₈N₆O₅

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Chemical Property of C₃₀H₃₈N₆O₅

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Technology Process of C₃₀H₃₈N₆O₅

There total 5 articles about C₃₀H₃₈N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29682-15-3
methyl 5-bromopicolinate

: 1401533-33-2
C₃₀H₃₈N₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / N,N-dimethyl-formamide / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 20 - 55 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 0.17 h

4.2: 3 h / 20 °C

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300214g

Reference yield:

: 852668-37-2
1-(4-aminophenyl)-3-(5-(tert-butyl)isoxazol-3-yl)urea

: 1268816-29-0
5-(1-(tert-butoxycarbonyl)piperidin-4-yl)picolinic acid

: 1401533-33-2
C₃₀H₃₈N₆O₅

Guidance literature:: 5-(1-(tert-butoxycarbonyl)piperidin-4-yl)picolinic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; for 0.166667h;

1-(4-aminophenyl)-3-(5-(tert-butyl)isoxazol-3-yl)urea; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1021/ml300214g

Reference yield:

: 375853-82-0,286961-14-6
tert-Butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

: 1401533-33-2
C₃₀H₃₈N₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / N,N-dimethyl-formamide / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 20 - 55 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 0.17 h

4.2: 3 h / 20 °C

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300214g