(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Base Information

Chemical Name:(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide
CAS No.:1616296-99-1
Molecular Formula:C₂₈H₃₅NO₃S
Molecular Weight:465.657
Hs Code.:

(R,R<sub>S</sub>)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Synonyms:(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Chemical Property:

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Technology Process of (R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

There total 5 articles about (R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1616296-98-0
(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]tertbutylsulfinamide

: 74-88-4
methyl iodide

: 1616296-99-1
(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Guidance literature:: (R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]tertbutylsulfinamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

methyl iodide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.04.044

Reference yield:

: 62932-96-1
(E)-1,2-dibenzyloxy-4-(2-nitroprop-1-en-1-yl)benzene

: 1616296-99-1
(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Guidance literature:: Multi-step reaction with 4 steps

1: iron; iron(III) chloride; hydrogenchloride / water; ethanol / 5 h / Reflux

2: titanium(IV) tetraethanolate / tetrahydrofuran / 5 h / Reflux

3: sodium tetrahydroborate / tetrahydrofuran / 3 h / -20 - 20 °C

4: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 20 °C

With hydrogenchloride; iron(III) chloride; titanium(IV) tetraethanolate; sodium tetrahydroborate; iron; sodium hydride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.04.044

Reference yield:

: 5447-02-9
3,4-dibenzyloxybenzaldehyde

: 1616296-99-1
(R,R_S)-N-[1-(3,4-dibenzyloxyphenyl)propan-2-yl]-N-methyltert-butylsulfinamide

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium acetate / 17 h / Reflux

2: iron; iron(III) chloride; hydrogenchloride / water; ethanol / 5 h / Reflux

3: titanium(IV) tetraethanolate / tetrahydrofuran / 5 h / Reflux

4: sodium tetrahydroborate / tetrahydrofuran / 3 h / -20 - 20 °C

5: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 20 °C

With hydrogenchloride; iron(III) chloride; titanium(IV) tetraethanolate; sodium tetrahydroborate; ammonium acetate; iron; sodium hydride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.04.044