5-fluoro-6-benzyloxy-7-chloronapthol-1

Base Information

Chemical Name:5-fluoro-6-benzyloxy-7-chloronapthol-1
CAS No.:1292322-40-7
Molecular Formula:C₁₇H₁₂ClFO₂
Molecular Weight:302.732
Hs Code.:

Synonyms:5-fluoro-6-benzyloxy-7-chloronapthol-1

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Chemical Property of 5-fluoro-6-benzyloxy-7-chloronapthol-1

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Technology Process of 5-fluoro-6-benzyloxy-7-chloronapthol-1

There total 7 articles about 5-fluoro-6-benzyloxy-7-chloronapthol-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₂ClFO₂

: 1292322-40-7
5-fluoro-6-benzyloxy-7-chloronapthol-1

Guidance literature:: C₁₈H₁₂ClFO₂; With 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In benzene; at 70 ℃; for 24h;

With hydrogenchloride; In water; benzene;

Reference yield:

: 2437-17-4
6-hydroxy-1-naphthoic acid

: 1292322-40-7
5-fluoro-6-benzyloxy-7-chloronapthol-1

Guidance literature:: Multi-step reaction with 8 steps

1: sulfuric acid / 80 °C

2: Selectfluor / acetonitrile / 3 h / 20 °C

3: zinc; acetic acid

4: SEC-BUTYLAMINE; sulfuryl dichloride / toluene / 3 h / 66 °C

5: potassium carbonate / acetonitrile / 2 h / Reflux

6: lithium aluminium tetrahydride / diethyl ether / 0.5 h

7: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

8: 3-chloro-benzenecarboperoxoic acid; potassium hydroxide / benzene / 24 h / 70 °C

With lithium aluminium tetrahydride; sulfuryl dichloride; SEC-BUTYLAMINE; sulfuric acid; potassium carbonate; acetic acid; Selectfluor; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; potassium hydroxide; zinc; In diethyl ether; dichloromethane; toluene; acetonitrile; benzene; 8: Baeyer-Villager;

Reference yield:

: 90162-13-3
methyl 6-hydroxy-1-naphthoate

: 1292322-40-7
5-fluoro-6-benzyloxy-7-chloronapthol-1

Guidance literature:: Multi-step reaction with 7 steps

1: Selectfluor / acetonitrile / 3 h / 20 °C

2: zinc; acetic acid

3: SEC-BUTYLAMINE; sulfuryl dichloride / toluene / 3 h / 66 °C

4: potassium carbonate / acetonitrile / 2 h / Reflux

5: lithium aluminium tetrahydride / diethyl ether / 0.5 h

6: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

7: 3-chloro-benzenecarboperoxoic acid; potassium hydroxide / benzene / 24 h / 70 °C

With lithium aluminium tetrahydride; sulfuryl dichloride; SEC-BUTYLAMINE; potassium carbonate; acetic acid; Selectfluor; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; potassium hydroxide; zinc; In diethyl ether; dichloromethane; toluene; acetonitrile; benzene; 7: Baeyer-Villager;