phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

Base Information

Chemical Name:phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester
CAS No.:859103-05-2
Molecular Formula:C₂₀H₂₆NO₆P
Molecular Weight:407.403
Hs Code.:

Synonyms:phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

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Chemical Property of phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

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Technology Process of phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

There total 4 articles about phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 859103-50-7
(3-benzyloxy-5-hydroxy)-N,N-diethylbenzamide

: 868-85-9
Dimethyl phosphite

: 859103-05-2
phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

Guidance literature:: With tetrachloromethane; dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at -10 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2005.04.104

Reference yield:

: 859103-01-8
(3,5-di-benzyloxy)-N,N-diethylbenzamide

: 859103-05-2
phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / hydrogen / Pd/C / acetic acid / 48 h

2: 92 percent / carbon tetrachloride; diisopropylethylamine; DMAP / acetonitrile / 0.5 h / -10 °C

With tetrachloromethane; dmap; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In acetic acid; acetonitrile; 2: Artherton-Todd reaction;
DOI:10.1016/j.tetlet.2005.04.104

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 859103-05-2
phosphoric acid (3-diethylcarbamoyl-5-benzyloxy-phenyl) ester dimethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

2: 100 percent / MeOH / aq. NaOH / 20 °C

3: 91 percent / BOP / tetrahydrofuran / 0.17 h / 20 °C

4: 66 percent / hydrogen / Pd/C / acetic acid / 48 h

5: 92 percent / carbon tetrachloride; diisopropylethylamine; DMAP / acetonitrile / 0.5 h / -10 °C

With methanol; tetrachloromethane; dmap; hydrogen; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; sodium hydroxide; acetic acid; N,N-dimethyl-formamide; acetonitrile; 5: Artherton-Todd reaction;
DOI:10.1016/j.tetlet.2005.04.104