1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Base Information

Chemical Name:1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide
CAS No.:339588-29-3
Molecular Formula:C₂₇H₄₁ClN₂O₁₀S₅
Molecular Weight:749.413
Hs Code.:

Synonyms:1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Suppliers and Price of 1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

There total 7 articles about 1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 57630-57-6
hexane-1,6-disulfonyl chloride

: 339588-28-2
1-[6-hexyl-N-(benzyl)sulfonamide]-N-(benzyl)methyldisulfonimide

: 339588-29-3
1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Guidance literature:: 1-[6-hexyl-N-(benzyl)sulfonamide]-N-(benzyl)methyldisulfonimide; With sodium hydride; In tetrahydrofuran; for 2h;

hexane-1,6-disulfonyl chloride; In tetrahydrofuran; Further stages.;
DOI:10.1021/ja002465v

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 339588-29-3
1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 89 percent / sodium sulfite / H₂O / 72 h / Heating

2.1: 78 percent / PCl₅ / 4 h / 90 °C

3.1: NaH / tetrahydrofuran / 1 h

3.2: 60 percent / tetrahydrofuran / 1 h

4.1: 92.4 percent / tetrahydrofuran / 1.5 h

5.1: NaH / tetrahydrofuran / 2 h

5.2: 36 percent / tetrahydrofuran

With phosphorus pentachloride; sodium hydride; sodium sulfite; In tetrahydrofuran; water;
DOI:10.1021/ja002465v

Reference yield:

: 109203-08-9
1,6-hexanedisulfonic acid disodium salt

: 339588-29-3
1-[1-(6-hexylsulfonyl chloride)-6-hexyl-N-(benzyl)hexyldisulfonimide]-N-benzylhexyldimethylsulfonimide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 78 percent / PCl₅ / 4 h / 90 °C

2.1: NaH / tetrahydrofuran / 1 h

2.2: 60 percent / tetrahydrofuran / 1 h

3.1: 92.4 percent / tetrahydrofuran / 1.5 h

4.1: NaH / tetrahydrofuran / 2 h

4.2: 36 percent / tetrahydrofuran

With phosphorus pentachloride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja002465v