Technology Process of C25H36N2O4S
There total 5 articles about C25H36N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: chlorosulfonic acid / dichloromethane / 0.75 h / 0 - 20 °C
2.1: water; ammonia / dichloromethane / 12 h / 20 °C
3.1: neat (no solvent) / 16 h / 160 °C
4.1: C28H26F6N4O / diethyl ether / 96 h / -10 °C
4.2: 0.5 h / 20 °C
5.1: water; sodium hydroxide / 3 h / 0 - 20 °C
With
chlorosulfonic acid; C28H26F6N4O; ammonia; water; sodium hydroxide;
In
diethyl ether; dichloromethane;
4.1: |Mannich Aminomethylation;
DOI:10.1002/adsc.201300135
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; ammonia / dichloromethane / 12 h / 20 °C
2.1: neat (no solvent) / 16 h / 160 °C
3.1: C28H26F6N4O / diethyl ether / 96 h / -10 °C
3.2: 0.5 h / 20 °C
4.1: water; sodium hydroxide / 3 h / 0 - 20 °C
With
C28H26F6N4O; ammonia; water; sodium hydroxide;
In
diethyl ether; dichloromethane;
3.1: |Mannich Aminomethylation;
DOI:10.1002/adsc.201300135