((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Base Information

Chemical Name:((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene
CAS No.:1204222-21-8
Molecular Formula:C₅₁H₄₉ClO₄
Molecular Weight:763.385
Hs Code.:

((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Synonyms:((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

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Chemical Property of ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

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Technology Process of ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

There total 5 articles about ((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204222-19-4
(1R,4R,5S,6R)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)-1-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-2-enol

: 1204222-21-8
((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -25 ℃;

Reference yield:

: 1204220-77-8
4-bromo-1-chloro-2-(4-cyclopropylbenzyl)benzene

: 1204222-21-8
((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammonium bisulfate; water-d2; sodium hydride / hexane / 0 - 25 °C

1.2: 0 - 20 °C

2.1: magnesium; ethylene dibromide / tetrahydrofuran / Reflux; Inert atmosphere

2.2: 3 h / 25 °C / Inert atmosphere

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -25 °C

With triethylsilane; tetrabutylammonium bisulfate; boron trifluoride diethyl etherate; water-d2; sodium hydride; magnesium; ethylene dibromide; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 1204220-70-1
(5-bromo-2-chlorophenyl)(4-cyclopropylphenyl)methanone

: 1204222-21-8
((1R,2S,3S,6R)-6-(benzyloxymethyl)-4-(4-chloro-3-((4-cyclopropylphenyl)methyl-d2)phenyl)cyclohex-4-ene-1,2,3-triyl)tris(oxy)tris(methylene)tribenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃SiD; trifluorormethanesulfonic acid; trifluoroacetic acid / tetrahydrofuran / 2 h / 25 °C

2.1: magnesium; ethylene dibromide / tetrahydrofuran / Reflux; Inert atmosphere

2.2: 3 h / 25 °C / Inert atmosphere

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -25 °C

With triethylsilane; Et₃SiD; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; magnesium; ethylene dibromide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;