farnesylfarnesylacetone

Base Information

• Chemical Name: farnesylfarnesylacetone
• CAS No.: 32304-17-9
• Molecular Formula: C₃₃H₅₄O
• Molecular Weight: 466.791

Synonyms:farnesylfarnesylacetone

Chemical Property of farnesylfarnesylacetone

Chemical Property:

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Technology Process of farnesylfarnesylacetone

There total 1 articles about farnesylfarnesylacetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3,5-dibromo-4-(di-tert-butyl(nonaprenyloxy)silyloxy)benzoic acid (1033756-53-4) → farnesylfarnesylacetone (32304-17-9) + geranylfarnesylacetone (86541-61-9) + C22H36O2 (869878-11-5) + 10-hydroxy-4,8-dimethyldeca-4,8-dienal (87920-55-6) + methyl 3,5-dibromo-4-hydroxybenzoate (41727-47-3) + (4E,8E,12E)-14-hydroxy-4,8,12-trimethyltetradeca-4,8,12-trienal (87920-56-7) + 5E,9E,13E-geranylgeranyl acetone (6809-52-5)

Guidance literature:

3,5-dibromo-4-(di-tert-butyl(nonaprenyloxy)silyloxy)benzoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 23 ℃; for 0.5h;

With dihydrogen peroxide; In dichloromethane; at -78 - -20 ℃;

diazomethane; With tetrabutylammonium periodite; pyridine hydrogenfluoride; periodic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water; Further stages;

DOI:10.1021/ja801899v

Reference yield:

farnesylfarnesylacetone (32304-17-9) → chlorobiumquinone (21884-42-4)

Guidance literature:

Multi-step reaction with 2 steps

2: AgO, H₃PO₄ / dioxane

With silver(II) oxide; phosphoric acid; In 1,4-dioxane;

DOI:10.1021/ja01052a081

Reference yield:

diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + farnesylfarnesylacetone (32304-17-9) → (2Ξ,6E,10E,14E,18E,22E,26E)-3,7,11,15,19,23,27-heptamethyl-octacosa-2,6,10,14,18,22,26-heptaen-1-ol (5905-41-9,13476-39-6,32247-55-5,32304-16-8,81338-25-2,89577-07-1,96647-65-3,102043-79-8)

Guidance literature:

Multistep reaction; (i) NaH, (ii) LiAlH₄, AlCl₃;

DOI:10.1021/jo00824a023

upstream raw materials:

diazomethane

3,5-dibromo-4-(di-tert-butyl(nonaprenyloxy)silyloxy)benzoic acid

Downstream raw materials:

(2Ξ,6E,10E,14E,18E,22E,26E)-3,7,11,15,19,23,27-heptamethyl-octacosa-2,6,10,14,18,22,26-heptaen-1-ol

chlorobiumquinone

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