C₅₆H₅₆N₆Si₂

Base Information

• Chemical Name: C₅₆H₅₆N₆Si₂
• CAS No.: 265670-94-8
• Molecular Formula: C₅₆H₅₆N₆Si₂
• Molecular Weight: 869.272
• Mol file: 265670-94-8.mol

Synonyms:C₅₆H₅₆N₆Si₂

Chemical Property of C₅₆H₅₆N₆Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₅₆N₆Si₂

There total 9 articles about C₅₆H₅₆N₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodophenylamine (615-43-0) → C56H56N6Si2 (265670-94-8)

Guidance literature:

Multi-step reaction with 5 steps

1.1: bis(triphenylphosphine)palladium(II)chloride; copper(I) iodide; triethylamine / 25 - 50 °C

2.1: iodomethane / 120 °C

3.1: 88 percent / copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

4.1: potassium carbonate / methanol; tetrahydrofuran

5.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

5.2: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; methyl iodide; In tetrahydrofuran; methanol; 1.1: Addition / 2.1: Decomposition / 3.1: Substitution / 4.1: Hydrolysis / 5.1: Substitution / 5.2: Substitution;

DOI:10.1021/ol005623w

Reference yield:

3,3-diethyl-1-(2-((trimethylsilyl)ethynyl)phenyl)triaz-1-ene (265670-90-4) → C56H56N6Si2 (265670-94-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: iodomethane / 120 °C

2.1: 88 percent / copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

3.1: potassium carbonate / methanol; tetrahydrofuran

4.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

4.2: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; methyl iodide; In tetrahydrofuran; methanol; 1.1: Decomposition / 2.1: Substitution / 3.1: Hydrolysis / 4.1: Substitution / 4.2: Substitution;

DOI:10.1021/ol005623w

Reference yield:

1-iodo-2-ethynylbenzene (137648-47-6) → C56H56N6Si2 (265670-94-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 88 percent / copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

2.1: potassium carbonate / methanol; tetrahydrofuran

3.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

3.2: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; 1.1: Substitution / 2.1: Hydrolysis / 3.1: Substitution / 3.2: Substitution;

DOI:10.1021/ol005623w

upstream raw materials:

trimethylsilylacetylene

2-iodophenylamine

1-iodo-2-ethynylbenzene

3,3-diethyl-1-(2-ethynylphenyl)triaz-1-ene