3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

Base Information

Chemical Name:3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine
CAS No.:131933-43-2
Molecular Formula:C₃₅H₃₂N₂O₄Se
Molecular Weight:623.61
Hs Code.:

Synonyms:3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

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Technology Process of 3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

There total 3 articles about 3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25442-42-6
5'-O-trityl-2,3'-anhydrothymidine

: 1666-13-3
diphenyl diselenide

: 131933-43-2
3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

Guidance literature:: With lithium aluminium tetrahydride; Yield given. Multistep reaction; 1) THF, 0 deg C, warm to RT over 0.25 h, 2) THF, reflux, 3 h; Na, THF, HMPA also used;
DOI:10.1021/jo00006a037

Reference yield:

: 25442-42-6
5'-O-trityl-2,3'-anhydrothymidine

: 1666-13-3
diphenyl diselenide

: 131933-43-2
3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

: 55612-11-8
5'-O-trityldeoxyxylothymidine

Guidance literature:: With sodium; Yield given. Multistep reaction. Yields of byproduct given; 1a) THF, reflux, 4 h, 1b) HMPA, heating, 3 h, 2) heating, 8 h;
DOI:10.1021/jo00006a037

Reference yield:

: 25442-42-6
5'-O-trityl-2,3'-anhydrothymidine

: 64-17-5
ethanol

: 1666-13-3
diphenyl diselenide

: 108441-77-6
2-ethoxy-1-(2-deoxy-5-O-trityl-β-D-threofuranosyl)thymine

: 131933-43-2
3'-α-(phenylselenyl)-5'-O-trityl-3'-deoxythymidine

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction. Yields of byproduct given; 2) reflux, 16 h;
DOI:10.1021/jo00006a037