C₅₉H₈₆O₁₆Si₂

Base Information

Chemical Name:C₅₉H₈₆O₁₆Si₂
CAS No.:929682-75-7
Molecular Formula:C₅₉H₈₆O₁₆Si₂
Molecular Weight:1107.49
Hs Code.:

C<sub>59</sub>H<sub>86</sub>O<sub>16</sub>Si<sub>2</sub>

Synonyms:C₅₉H₈₆O₁₆Si₂

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Chemical Property of C₅₉H₈₆O₁₆Si₂

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Technology Process of C₅₉H₈₆O₁₆Si₂

There total 20 articles about C₅₉H₈₆O₁₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929682-64-4
C₅₉H₈₄O₁₆Si₂

: 929682-75-7
C₅₉H₈₆O₁₆Si₂

Guidance literature:: With hydrogen; RhCl(PPh₃)3; In ethanol; under 760 Torr;
DOI:10.1021/ja068901g

Reference yield:

: 929682-57-5
2-methyl-but-2-enoic acid 7-hydroxy-2-(4-methoxy-phenyl)-6-[2,2,4-trimethyl-6-(1-propyl-but-3-enyloxy)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy]-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 929682-75-7
C₅₉H₈₆O₁₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96 percent / 2,6-lutidine / CH₂Cl₂ / 2 h

2.1: molecular sieves 4 Angstroem; NaBH₃CN; TMSCl / acetonitrile / 0 - 20 °C

2.2: 56.8 mg / DMAP / toluene; CH₂Cl₂ / 3 h

3.1: DDQ; water / CH₂Cl₂ / 16 h / 20 °C

4.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / toluene / 1.5 h / 20 °C

4.2: 54.6 mg / DMAP / toluene / 2 h

5.1: RuCl₂(IMes)(PCy₃)=CHPh / CH₂Cl₂ / 4 h / Heating

6.1: 60 mg / H₂ / RhCl(PPh₃)3 / ethanol / 760 Torr

With 2,6-dimethylpyridine; chloro-trimethyl-silane; 4 A molecular sieve; 2,4,6-trichlorobenzoyl chloride; water; hydrogen; sodium cyanoborohydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene](benzylidene)Ru(II) dichloride; RhCl(PPh₃)3; In ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja068901g

Reference yield:

: 98-01-1
furfural

: 929682-75-7
C₅₉H₈₆O₁₆Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: Mg; 1,2-dibromoethane / tetrahydrofuran / 1 h / 20 °C

1.2: 82 percent / tetrahydrofuran / 2 h / 0 °C

2.1: 47 percent / Ti(OiPr)4; D-(-)-diisopropyl tartrate; t-BuOOH / CH₂Cl₂; decane / 24 h / -20 °C

3.1: 71 percent / VO(acac)2; t-BuOOH / CH₂Cl₂; decane / 3 h / 20 °C

4.1: CrO₃; H₂SO₄ / acetone / 3 h / 20 °C

5.1: 324 mg / Zn; AcOH / CHCl₃ / 3 h / 20 °C

6.1: p-TsOH*H₂O / CH₂Cl₂ / 15 h

7.1: 156 mg / triethylamine / DMAP / CH₂Cl₂ / 3 h

8.1: 68 percent / TASF / dimethylformamide / 3 h

9.1: 2,4,6-trichlorobenzoyl chloride; Et₃N / toluene / 1.5 h / 20 °C

9.2: 54.6 mg / DMAP / toluene / 2 h

10.1: RuCl₂(IMes)(PCy₃)=CHPh / CH₂Cl₂ / 4 h / Heating

11.1: 60 mg / H₂ / RhCl(PPh₃)3 / ethanol / 760 Torr

With chromium(VI) oxide; titanium(IV) isopropylate; tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; sulfuric acid; 2,4,6-trichlorobenzoyl chloride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; hydrogen; D-(-)-diisopropyl tartrate; magnesium; acetic acid; ethylene dibromide; triethylamine; zinc; dmap; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene](benzylidene)Ru(II) dichloride; RhCl(PPh₃)3; toluene-4-sulfonic acid; In tetrahydrofuran; decane; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetone; toluene; 4.1: Jones' oxidation;
DOI:10.1021/ja068901g