succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

Base Information

Chemical Name:succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate
CAS No.:389119-36-2
Molecular Formula:C₁₉H₂₅N₃O₇
Molecular Weight:407.423
Hs Code.:

Synonyms:succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

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Chemical Property of succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

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Technology Process of succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

There total 5 articles about succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: (2-benzyloxy-1-isocyanato-ethyl)-carbamic acid tert-butyl ester

: 389119-36-2
succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

Guidance literature:: In toluene; at 65 ℃; for 0.0833333h;
DOI:10.1021/ol0166552

Reference yield:

: 23680-31-1
BOC-O-benzyl-L-serine

: 389119-36-2
succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: NMM / tetrahydrofuran / -20 - -5 °C

2: NaN₃ / H₂O; tetrahydrofuran / 0.08 h / -5 °C

3: toluene / 0.17 h / 65 °C

4: toluene / 0.08 h / 65 °C

With 4-methyl-morpholine; sodium azide; In tetrahydrofuran; water; toluene; 3: Curtius rearrangement;
DOI:10.1021/ol0166552

Reference yield:

: (C₅H₉O₂)(NHCHCOO)(CH₂OC₇H₇)(CO₂C₂H₅)

: 389119-36-2
succinimidyl N-[2-benzyloxy-1-(tert-butoxycarbonylamino)ethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / H₂O; tetrahydrofuran / 0.08 h / -5 °C

2: toluene / 0.17 h / 65 °C

3: toluene / 0.08 h / 65 °C

With sodium azide; In tetrahydrofuran; water; toluene; 2: Curtius rearrangement;
DOI:10.1021/ol0166552