Technology Process of threo-3,4-epoxy-2-octanyl tosylate
There total 3 articles about threo-3,4-epoxy-2-octanyl tosylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
diethyl ether;
-10 deg C, 20 min, then -10 deg C, 1 h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / 85percent m-chloroperbenzoic acid / CH2Cl2 / 0 deg C, then Rt, 2 h
2: 83 percent / powdered KOH / diethyl ether / -10 deg C, 20 min, then -10 deg C, 1 h
With
potassium hydroxide; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / Ni(OAc)2*4H2O, NaBH4, 2 M aq. NaOH, ethylenediamine / aq. ethanol / 4 h
2: 95 percent / 85percent m-chloroperbenzoic acid / CH2Cl2 / 0 deg C, then Rt, 2 h
3: 83 percent / powdered KOH / diethyl ether / -10 deg C, 20 min, then -10 deg C, 1 h
With
potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; nickel diacetate; ethylenediamine; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; ethanol; dichloromethane;
