11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

Base Information

Chemical Name:11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one
CAS No.:1433704-68-7
Molecular Formula:C₂₇H₂₅NO₂
Molecular Weight:395.501
Hs Code.:

Synonyms:11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

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Chemical Property of 11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

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Technology Process of 11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

There total 2 articles about 11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 126-81-8
dimedone

: 95-55-6
2-amino-phenol

: 3218-36-8
4-Phenylbenzaldehyde

: 1433704-68-7
11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

Guidance literature:: With choline chloride; urea; at 80 ℃;
DOI:10.1016/j.tetlet.2016.07.005

Reference yield: 65.0%

: 504-02-9
1,3-cylohexanedione

: 95-55-6
2-amino-phenol

: 3218-36-8
4-Phenylbenzaldehyde

: 1433704-68-7
11-([1,1'-biphenyl]-4-yl)-3,3-dimethyl-3,4,5,11-tetrahydrodibenzo[b,e][1,4]oxazepin-1(2H)-one

Guidance literature:: 1,3-cylohexanedione; 2-amino-phenol; In 1,2-dichloro-ethane; for 4h; Reflux;

4-Phenylbenzaldehyde; With trifluoroacetic acid; In 1,2-dichloro-ethane; for 24h; Reflux;
DOI:10.1016/j.tetlet.2013.03.131