2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

Base Information

Chemical Name:2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester
CAS No.:1309367-37-0
Molecular Formula:C₂₇H₂₅N₃OS₂
Molecular Weight:471.647
Hs Code.:

Synonyms:2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

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Chemical Property of 2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

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Technology Process of 2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

There total 4 articles about 2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-15-0,12122-00-8
carbon disulfide

: 39186-58-8
4-bromo-2,2-diphenylbutyronitrile

: 5368-28-5
2-phenyl-3-keto-piperazine

: 1309367-37-0
2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

Guidance literature:: 2-phenyl-3-keto-piperazine; With potassium phosphate; In acetone; at 20 ℃; for 0.25h;

carbon disulfide; In acetone;

4-bromo-2,2-diphenylbutyronitrile; In acetone;
DOI:10.1002/ardp.201000259

Reference yield:

: 86-29-3
Diphenylacetonitrile

: 1309367-37-0
2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; sodium hydroxide / water

2: potassium phosphate / acetone / 0.25 h / 20 °C

With potassium phosphate; tetrabutylammomium bromide; sodium hydroxide; In water; acetone;
DOI:10.1002/ardp.201000259

Reference yield:

: 103-82-2
phenylacetic acid

: 1309367-37-0
2-phenyl-3-oxo-piperazine-1-carbodithioic acid 3-cyano-3,3-diphenylpropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; phosphorus trichloride / Reflux

2: ethanol / Reflux

3: potassium phosphate / acetone / 0.25 h / 20 °C

With potassium phosphate; bromine; phosphorus trichloride; In ethanol; acetone;
DOI:10.1002/ardp.201000259