(+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

Base Information

Chemical Name:(+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate
CAS No.:1235994-60-1
Molecular Formula:C₂₀H₂₁F₂NO₃S
Molecular Weight:393.454
Hs Code.:

Synonyms:(+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

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Technology Process of (+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

There total 1 articles about (+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1235994-59-8
(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

: 1235994-60-1
(+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol101318t