(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

Base Information

Chemical Name:(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate
CAS No.:1235994-59-8
Molecular Formula:C₂₂H₂₅F₂NO₃S
Molecular Weight:421.508
Hs Code.:

Synonyms:(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

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Chemical Property of (+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

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Technology Process of (+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

There total 1 articles about (+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1235994-43-0
(+)-methyl 6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

: 106-95-6
allyl bromide

: 1235994-59-8
(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

Guidance literature:: (+)-methyl 6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101318t

Reference yield: 80.0%

: 1235994-59-8
(+)-methyl N-allyl-6-(1,1-difluorobut-3-enyl)-4-[(R)-p-tolylsulfinylmethyl]-1,4-dihydropyridin-3-carboxylate

: 1235994-60-1
(+)-methyl 10,10-difluoro-2-[(R)-p-tolylsulfinylmethyl]-2,6,9,10-tetrahydropyrido[1,2-a]azepine-3-carboxylate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol101318t