3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

Base Information

Chemical Name:3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine
CAS No.:133832-64-1
Molecular Formula:C₂₇H₂₄N₄O₇
Molecular Weight:516.51
Hs Code.:

Synonyms:3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

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Chemical Property of 3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

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Technology Process of 3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

There total 3 articles about 3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 109151-82-8
7-nitro-3H-imidazo<4,5-b>pyridine

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 133832-64-1
3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

: 175908-27-7
1-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-1H-imidazo<4,5-b>pyridine

Guidance literature:: With potassium hydroxide; Tris(3,6-dioxaheptyl)amine; In acetonitrile; for 0.333333h; Ambient temperature;
DOI:10.1002/hlca.19960790117

Reference yield:

: 109151-82-8
7-nitro-3H-imidazo<4,5-b>pyridine

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 133832-64-1
3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) acetonitrile, RT, 30 min, 2.) acetonitrile, 0 deg C, 3 h;
DOI:10.1021/jm00111a044

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 109151-82-8
7-nitro-3H-imidazo[4,5-b]pyridine

: 133832-64-1
3-<2-deoxy-3,5-di-O-(4-toluoyl)-β-D-erythro-pentofuranosyl>-7-nitro-3H-imidazo<4,5-b>pyridine

Guidance literature:: With tin(IV) chloride; sodium hydride; Yield given. Multistep reaction; 1) CH₃CN, 0.5 h, 2) CH₃CN, 16 h, 25 deg C;
DOI:10.1016/0040-4039(95)00098-W