Technology Process of C54H97I3O10SSi3
There total 8 articles about C54H97I3O10SSi3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 2,2'-dipyridyl carbonate;
In
dichloromethane;
at 20 ℃;
for 48h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; pyridine / 16 h / 20 °C
2: 2,6-dimethylpyridine / dichloromethane / 16 h / Inert atmosphere
3: ethanol / 3 h / Reflux
4: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 22 h / 20 °C
5: pyridine / dichloromethane / 2 h / 20 °C
6: dmap; 2,2'-dipyridyl carbonate / dichloromethane / 48 h / 20 °C
With
pyridine; 2,6-dimethylpyridine; dmap; 2,2'-dipyridyl carbonate; trimethylamine-N-oxide; water;
osmium(VIII) oxide;
In
ethanol; dichloromethane; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: trifluorormethanesulfonic acid / 48 h / 0 - 80 °C
1.2: 4 h / 40 °C
2.1: water; acetic acid / 1 h / 100 °C
3.1: dmap; pyridine / 16 h / 20 °C
4.1: 2,6-dimethylpyridine / dichloromethane / 16 h / Inert atmosphere
5.1: ethanol / 3 h / Reflux
6.1: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 22 h / 20 °C
7.1: pyridine / dichloromethane / 2 h / 20 °C
8.1: dmap; 2,2'-dipyridyl carbonate / dichloromethane / 48 h / 20 °C
With
pyridine; 2,6-dimethylpyridine; dmap; 2,2'-dipyridyl carbonate; trimethylamine-N-oxide; trifluorormethanesulfonic acid; water; acetic acid;
osmium(VIII) oxide;
In
ethanol; dichloromethane; tert-butyl alcohol;