<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

Base Information

Chemical Name:<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal
CAS No.:87011-67-4
Molecular Formula:C₁₅H₂₇NO₂
Molecular Weight:253.385
Hs Code.:

Synonyms:<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

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Chemical Property of <(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

Chemical Property:

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Technology Process of <(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

There total 5 articles about <(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87011-66-3
(3R,4S)-3-(4,4-Dimethoxy-butyl)-2-dimethylaminomethyl-3,4-dimethyl-cyclohexanone

: 87011-67-4
<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

Guidance literature:: With hydrogenchloride; for 0.25h; Ambient temperature;
DOI:10.1021/jo00168a067

Reference yield:

: 10463-42-0
3,4-dimethyl-cyclohex-2-enone

: 87011-67-4
<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg; 2.) copper(I) iodide / 1.) ether, RT_., 15 min; 2.) dimethyl sufide, ether, 0 deg C, then rt.; 3.) 0 deg C, 2 h, rt. 12 h

2: 1.) ozone; 2.) p-toluenesulfonic acid / 1.) CH₂Cl₂, MeOH, -78 deg C, 4 h; 2.) 1 h, rt.

3: 1.) acetyl chloride; MeLi / 1.) ether, rt.; 2.) THF, -78 deg C, 15 min, then 2 h

4: 0.65 N HCl

With hydrogenchloride; copper(l) iodide; methyllithium; toluene-4-sulfonic acid; ozone; magnesium; acetyl chloride;
DOI:10.1021/ja00294a046

Reference yield:

: 87011-65-2
methyl (trans-3,4-dimethoxybutyl-3-(4-pentenyl)-1-cyclohexen-1-yl)-carbonate

: 87011-67-4
<(1α,6β)-2-<(dimethylamino)methyl>-1,6-dimethyl-3-oxo-cyclohexanyl>butanal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) acetyl chloride; MeLi / 1.) ether, rt.; 2.) THF, -78 deg C, 15 min, then 2 h

2: 0.65 N HCl

With hydrogenchloride; methyllithium; acetyl chloride;
DOI:10.1021/ja00294a046