N-phenyl-2-hydroxyproanesulfonamide mesylate

Base Information

Chemical Name:N-phenyl-2-hydroxyproanesulfonamide mesylate
CAS No.:265995-52-6
Molecular Formula:C₁₀H₁₅NO₅S₂
Molecular Weight:293.365
Hs Code.:

Synonyms:N-phenyl-2-hydroxyproanesulfonamide mesylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-2-hydroxyproanesulfonamide mesylate

Chemical Property:

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Technology Process of N-phenyl-2-hydroxyproanesulfonamide mesylate

There total 3 articles about N-phenyl-2-hydroxyproanesulfonamide mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 265995-46-8
N-phenyl-2-hydroxypropanesulfonamide

: 265995-52-6
N-phenyl-2-hydroxyproanesulfonamide mesylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ja994293b

Reference yield:

: 2225-19-6
N-phenyl-S-ethylsulfonamide

: 265995-52-6
N-phenyl-2-hydroxyproanesulfonamide mesylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi; TMEDA / hexane; tetrahydrofuran / 2 h / 20 °C

1.2: hexane; tetrahydrofuran

2.1: Et₃N / CH₂Cl₂ / 2 h / 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 1.1: Metallation / 1.2: Addition / 2.1: mesylation;
DOI:10.1021/ja994293b

Reference yield:

: 62-53-3
aniline

: 265995-52-6
N-phenyl-2-hydroxyproanesulfonamide mesylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 2 h / Heating

2.1: n-BuLi; TMEDA / hexane; tetrahydrofuran / 2 h / 20 °C

2.2: hexane; tetrahydrofuran

3.1: Et₃N / CH₂Cl₂ / 2 h / 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; In tetrahydrofuran; hexane; dichloromethane; toluene; 1.1: amidation / 2.1: Metallation / 2.2: Addition / 3.1: mesylation;
DOI:10.1021/ja994293b