(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

Base Information

Chemical Name:(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate
CAS No.:1374153-68-0
Molecular Formula:CF₃O₃S*C₁₈H₂₂FS
Molecular Weight:438.507
Hs Code.:

Synonyms:(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

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Chemical Property of (fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

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Technology Process of (fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

There total 4 articles about (fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.44%

: 358-23-6
trifluoromethylsulfonic anhydride

: 488-23-3
1,2,3,4-Tetramethylbenzene

: 65325-67-9,338996-18-2
1-((fluoromethyl)sulfinyl)-4-methylbenzene

: 1374153-68-0
(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

Guidance literature:: In diethyl ether; at -10 ℃; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 65325-64-6
1-[(fluoromethyl)sulfanyl]-4-methylbenzene

: 1374153-68-0
(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / water; methanol / 0 - 5 °C

2: diethyl ether / -10 °C / Inert atmosphere

With N-Bromosuccinimide; In methanol; diethyl ether; water;

Reference yield:

: 623-13-2
4-methylphenyl methylsulfide

: 1374153-68-0
(fluoromethyl)(2,3,4,5-tetramethylphenyl)(p-tolyl)sulfonium triflate

Guidance literature:: Multi-step reaction with 4 steps

1: N-chloro-succinimide / chlorobenzene / 35 - 45 °C / Inert atmosphere

2: cesium fluoride / PEG₄₀₀ / 80 - 85 °C / Inert atmosphere

3: N-Bromosuccinimide / water; methanol / 0 - 5 °C

4: diethyl ether / -10 °C / Inert atmosphere

With N-chloro-succinimide; N-Bromosuccinimide; cesium fluoride; In methanol; PEG₄₀₀; diethyl ether; water; chlorobenzene;