3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Base Information

Chemical Name:3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde
CAS No.:332940-64-4
Molecular Formula:C₁₈H₂₂O₃
Molecular Weight:286.371
Hs Code.:

Synonyms:3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Suppliers and Price of 3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

There total 2 articles about 3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 332940-62-2
[3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propenyl]-(4-methoxy-phenyl)-carbamic acid tert-butyl ester

: 332940-64-4
3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Guidance literature:: With hydrogenchloride; In chloroform;
DOI:10.1021/ol007012+

Reference yield:

: 332940-60-0
(4-methoxy-phenyl)-[3-(3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propenyl]-carbamic acid tert-butyl ester

: 332940-64-4
3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: 81 percent / tetrahydrofuran / -78 °C

2.1: 79 percent / aq. HCl / CHCl₃

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1021/ol007012+

Reference yield: 86.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 332940-64-4
3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde

: 332940-66-6
3-allyl-3-methyl-4-(1-phenyl-but-3-enyl)-tetrahydro-pyran-2-one

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at -78 ℃;

3-(3-allyl-3-methyl-2-oxo-tetrahydro-pyran-4-yl)-3-phenyl-propionaldehyde; In tetrahydrofuran; Further stages.;
DOI:10.1021/ol007012+