methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

Base Information

Chemical Name:methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate
CAS No.:1237519-36-6
Molecular Formula:C₃₅H₃₅N₃O₇
Molecular Weight:609.679
Hs Code.:

Synonyms:methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

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Chemical Property of methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

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Technology Process of methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

There total 4 articles about methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237518-23-8
methyl 2-amino-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

: 2-acetoxy-5-(pyridin-3-yl)benzoic acid chloride

: 1237519-36-6
methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃; for 1.66667h; Cooling with ice;

Reference yield:

: 1237518-30-7
2-acetoxy-5-(pyridin-3-yl)benzoic acid

: 1237519-36-6
methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: pyridine / tetrahydrofuran / 1.67 h / 20 °C / Cooling with ice

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 201662-55-7
2-(benzyloxy)-5-(pyridin-3-yl)benzoic acid

: 1237519-36-6
methyl 2-(2-acetoxy-5-(pyridin-3-yl)benzamido)-4-(2-((tert-butoxycarbonyl)(ethyl)amino)phenyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / 3 h / 20 °C

2: pyridine / dichloromethane / 1.5 h / Reflux

3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: pyridine / tetrahydrofuran / 1.67 h / 20 °C / Cooling with ice

With pyridine; oxalyl dichloride; trifluoroacetic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;