sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

Base Information

Chemical Name:sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate
CAS No.:1237514-83-8
Molecular Formula:C₂₇H₂₂N₃O₄*Na
Molecular Weight:475.479
Hs Code.:

Synonyms:sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

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Chemical Property of sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

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Technology Process of sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

There total 8 articles about sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237519-37-7
4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoic acid

: 1237514-83-8
sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 2.5h;

Reference yield:

: (x)C₂HF₃O₂*C₃₀H₂₇N₃O₅

: 1237514-83-8
sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

Guidance literature:: (x)C₂HF₃O₂*C₃₀H₂₇N₃O₅; With water; sodium hydroxide; In 1,4-dioxane; at 50 - 55 ℃; for 2h;

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃; pH=7.4;

With sodium hydroxide; In ethanol; water; at 20 ℃; for 2.5h;

Reference yield:

: 1237518-30-7
2-acetoxy-5-(pyridin-3-yl)benzoic acid

: 1237514-83-8
sodium 4-(2-(ethylamino)phenyl)-2-(2-hydroxy-5-(pyridin-3-yl)benzamido)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2.1: pyridine / tetrahydrofuran / 1.67 h / 20 °C / Cooling with ice

3.1: trifluoroacetic acid / 2.5 h / 20 °C

3.2: 2 h / 50 - 55 °C

3.3: pH 7.4

4.1: sodium hydroxide / ethanol; water / 2.5 h / 20 °C

With pyridine; oxalyl dichloride; trifluoroacetic acid; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; water;