C₃₄H₃₇N₃O₉

Base Information

Chemical Name:C₃₄H₃₇N₃O₉
CAS No.:1359021-91-2
Molecular Formula:C₃₄H₃₇N₃O₉
Molecular Weight:631.682
Hs Code.:

C<sub>34</sub>H<sub>37</sub>N<sub>3</sub>O<sub>9</sub>

Synonyms:C₃₄H₃₇N₃O₉

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Chemical Property of C₃₄H₃₇N₃O₉

Chemical Property:

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Technology Process of C₃₄H₃₇N₃O₉

There total 16 articles about C₃₄H₃₇N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359021-90-1
C₄₅H₅₉N₃O₁₁Si

: 1359021-91-2
C₃₄H₃₇N₃O₉

Guidance literature:: C₄₅H₅₉N₃O₁₁Si; With hydrogen fluoride; In tetrahydrofuran; water; at 20 ℃;

With dipotassium hydrogenphosphate; In tetrahydrofuran; water;

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359021-91-2
C₃₄H₃₇N₃O₉

Guidance literature:: Multi-step reaction with 16 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

8.2: 0.33 h / 20 °C

9.1: potassium carbonate / acetone / 2 h / Reflux

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -100 °C

10.2: 3 h / -100 - -78 °C

10.3: -78 °C

11.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

12.1: hydrogen / palladium on activated carbon / methanol / 2 h / 760.05 Torr / Sealed vessel

13.1: acetic acid; triethylamine / 1,2-dichloro-ethane / 2 h / 20 °C

13.2: 2 h / 20 °C

14.1: dmap / dichloromethane / 1 h / 20 °C

15.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C

15.2: 0.5 h / -100 - -10 °C

16.1: hydrogen fluoride / tetrahydrofuran; water / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; hydrogen fluoride; hydrogen; bromine; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; sodium nitrite; dmap; palladium on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359021-91-2
C₃₄H₃₇N₃O₉

Guidance literature:: Multi-step reaction with 14 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: potassium carbonate / acetone / 2 h / Reflux

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -100 °C

8.2: 3 h / -100 - -78 °C

8.3: -78 °C

9.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

10.1: hydrogen / palladium on activated carbon / methanol / 2 h / 760.05 Torr / Sealed vessel

11.1: acetic acid; triethylamine / 1,2-dichloro-ethane / 2 h / 20 °C

11.2: 2 h / 20 °C

12.1: dmap / dichloromethane / 1 h / 20 °C

13.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C

13.2: 0.5 h / -100 - -10 °C

14.1: hydrogen fluoride / tetrahydrofuran; water / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; hydrogen fluoride; hydrogen; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; dmap; palladium on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; toluene; tert-butyl alcohol;