[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

Base Information

Chemical Name:[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene
CAS No.:1204306-79-5
Molecular Formula:C₇H₈*C₅₀H₆₂FeN₅Si₂Y
Molecular Weight:1026.14
Hs Code.:

Synonyms:[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

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Chemical Property of [(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

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Technology Process of [(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

There total 1 articles about [(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1204306-92-2
[(1,1'-ferrocenylene(NSitBuMe₂)2)Y(tetrahydrofuran)(C₉H₇N(CH₂Ph))]

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1227476-15-4
Azobenzene

: 1204306-79-5
[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

Guidance literature:: In toluene; byproducts: C4H8O; (N2); stirring mixt. of yttrium compd. and azobenzene in toluene at 50°C for 24 h; evapn., dissolving in n-pentane, keeping at -35°C overnight, isolation of ppt., NMR;
DOI:10.1021/ja908489p

Reference yield: 55.2%

: 119-65-3
isoquinoline

: 1204306-79-5
[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(1-benzylisoquinoline)(η2-PhNNHPh)]*toluene

: 1204306-98-8
[(1,1'-ferrocenylene(NSi(tBu)Me2)2)Y(isoquinoline)2(η2-PhNNHPh)]

Guidance literature:: In toluene; (N2); stirring 1:2 mixt. of yttrium compd. and isoquinoline in toluene at 50°C for 2 h; evapn., dissolving in n-pentane, keeping at -35°C overnight, isolation of ppt., elem. anal.;
DOI:10.1021/ja908489p