methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:226927-52-2
Molecular Formula:C₃₃H₃₈N₆O₈
Molecular Weight:646.7
Hs Code.:

Synonyms:methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Chemical Property of methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 7 articles about methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20672-67-7
methyl 3,4,6-tri-O-benzyl-α-D-mannopyranoside

: 226927-52-2
methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: TMSOTf / acetonitrile / -40 °C

2: NaOMe

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; In acetonitrile;
DOI:10.1021/ja984062p

Reference yield:

: 226927-44-2
methyl 2,4-diazido-2,4-dideoxy-β-D-xylopyranoside

: 226927-52-2
methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / H₂SO₄

2: H₂NNH₂*AcOH / dimethylformamide / 50 °C

3: Cs₂CO₃ / 1,2-dichloro-ethane

4: TMSOTf / acetonitrile / -40 °C

5: NaOMe

With trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sodium methylate; hydrazinium monoacetate; caesium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja984062p

Reference yield:

: Acetic acid (3R,4S,5R)-3,5-diazido-2-hydroxy-tetrahydro-pyran-4-yl ester

: 226927-52-2
methyl (2,4-diazido-2,4-dideoxy-β-D-xylopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Cs₂CO₃ / 1,2-dichloro-ethane

2: TMSOTf / acetonitrile / -40 °C

3: NaOMe

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; caesium carbonate; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ja984062p