4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

Base Information

Chemical Name:4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile
CAS No.:69194-94-1
Molecular Formula:C₁₉H₂₄N₂O₃
Molecular Weight:328.411
Hs Code.:

Synonyms:4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

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Chemical Property of 4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

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Technology Process of 4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

There total 5 articles about 4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 4542-47-6
3-Morpholin-4-yl-propionitrile

: 69194-92-9
3,5-dimethoxy-4-(methylethenyl)benzaldehyde

: 69194-94-1
4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; at 75 ℃; for 0.25h;

Reference yield:

: 33187-98-3
3,5-dimethoxy-4-(methoxycarbonyl)benzaldehyde

: 69194-94-1
4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

Guidance literature:: Multi-step reaction with 4 steps

1: conc. HCl / ethanol / 2 h / Heating

2: diethyl ether / 3 h / Heating

3: H+

4: 81 percent / sodium methylate / dimethylformamide / 0.25 h / 75 °C

With hydrogenchloride; sodium methylate; hydrogen cation; In diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 16849-68-6
dimethyl 2,6-dimethoxyterephthalate

: 69194-94-1
4-isopropenyl-3,5-dimethoxy-α-(morpholinomethylene)-dihydrocinnamic acid nitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / sodium bis(2-methoxyethoxy)aluminum hyride, morpholine / toluene / 4 h / -15 °C

2: conc. HCl / ethanol / 2 h / Heating

3: diethyl ether / 3 h / Heating

4: H+

5: 81 percent / sodium methylate / dimethylformamide / 0.25 h / 75 °C

With morpholine; hydrogenchloride; sodium methylate; hydrogen cation; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;