benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

Base Information

Chemical Name:benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate
CAS No.:1430196-52-3
Molecular Formula:C₄₆H₆₄O₁₀
Molecular Weight:777.008
Hs Code.:

Synonyms:benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

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Chemical Property of benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

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Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

There total 3 articles about benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1430196-46-5
3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyl chloride

: 105730-97-0
benzyl 3α,7α,12α-trihydroxyl-5β-cholestane-24-carboxylic ester

: 1430196-52-3
benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.steroids.2013.02.001

Reference yield:

: 2050-25-1,1201808-31-2
diethylene glycol monobenzyl ether

: 1430196-52-3
benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / 1 h / 22 °C

2: oxalyl dichloride / toluene / 0.5 h / 22 °C

3: dmap / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1016/j.steroids.2013.02.001

Reference yield:

: 1430196-45-4
3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoic acid

: 1430196-52-3
benzyl 3α-{3-[2-(2-benzyloxyethoxy)ethoxycarbonyl]propanoyloxy}-7α,12α-dihydroxy-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / toluene / 0.5 h / 22 °C

2: dmap / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1016/j.steroids.2013.02.001